Synthesis new organic azo dye as reagent 3-((4-acetyl-3-hydroxyphenyl) diazenyl)-4-amino-N-(pyrimidin-2-yl)benzene sulfonamide (SDA) and Analytical Study of Co(II), Ni(II) and Cu(II),  metals complexes .The reagent and its complexes were characterized by elemental analysis, Uv-Vis, FT- IR and molar conductivity measurements. The data show that the complexes have the composition of [MR]X2 type. The conductivity data for all complexes are consistent with those expected for an electrolyte. Octahedral environment is suggested for metal complexes.